Polishing composition for magnetic disk substrate

Bibliographic Details
Title: Polishing composition for magnetic disk substrate
Document Number: 20070254563
Publication Date: November 1, 2007
Appl. No: 11/790615
Application Filed: April 26, 2007
Abstract: A polishing composition for a magnetic disk substrate of the present invention includes water, silica particles, and at least one or more selected from an acid, a salt of the acid, and an oxidizing agent. The silica particles are observed with a transmission electron microscope to measure a maximum diameter and a projected area of each particle, and a value obtained by dividing the area of a circle whose diameter is the maximum diameter of a silica particle by the projected area of the silica particle and multiplying the result by 100, is in the range of 100 to 130.
Inventors: Oshima, Yoshiaki (Wakayama, JP); Yamaguchi, Norihito (Wakayama, JP); Doi, Haruhiko (Wakayama, JP)
Claim: 1. A polishing composition for a magnetic disk substrate comprising: water; silica particles; and at least one or more selected from the group consisting of an acid, a salt of the acid, and an oxidizing agent, wherein the silica particles have a value in the range of 100 to 130, wherein the value is obtained by dividing an area of a circle whose diameter is the maximum diameter of the silica particle by the projected area of the silica particle and multiplying the result by 100, when observed with a transmission electron microscope to measure the maximum diameter and the projected area of each particle.
Claim: 2. The polishing composition according to claim 1, wherein in a graph of particle size versus cumulative volume frequency obtained by plotting a cumulative volume frequency (%) of the silica particles from a smaller particle size side against a particle size (nm) of the silica particles measured by transmission electron microscope observation, the cumulative volume frequency (V) and the particle size (R) satisfy the following formula (1): V≧0.5×R+40   (1) where R is in a range of 40 to 100 nm, and the cumulative volume frequency of the silica particles with a particle size of 15 nm is 20% or less.
Claim: 3. The polishing composition according to claim 1, wherein the silica particles are colloidal silica.
Claim: 4. The polishing composition according to claim 1, wherein an acid value of the polishing composition is 10 mgKOH/g or less.
Claim: 5. The polishing composition according to claim 1, wherein a content of the oxidizing agent is 0.1 to 1 wt %.
Claim: 6. The polishing composition according to claim 1, wherein the silica particles have a value in the range of 100 to 130, and the value is obtained by dividing an area of a circle whose circumference is a perimeter of the silica particle by the projected area of the silica particle and multiplying the result by 100, when observed with a transmission electron microscope to measure the perimeter and the projected area of each particle.
Claim: 7. A method for manufacturing a magnetic disk substrate comprising: a step of polishing a substrate to be polished with a polishing composition comprising water, silica particles, and at least one or more selected from the group consisting of an acid, a salt of the acid, and an oxidizing agent, wherein the silica particles have a value in the range of 100 to 130, wherein the value is obtained by dividing an area of a circle whose diameter is the maximum diameter of the silica particle by the projected area of the silica particle and multiplying the result by 100, when observed with a transmission electron microscope to measure the maximum diameter and the projected area of each particle.
Claim: 8. The method according to claim 7, wherein in a graph of particle size versus cumulative volume frequency obtained by plotting a cumulative volume frequency (%) of the silica particles from a smaller particle size side against a particle size (nm) of the silica particles measured by transmission electron microscope observation, the cumulative volume frequency (V) and the particle size (R) satisfy the following formula (1): V≧0.5×R+40   (1) where R is in a range of 40 to 100 nm, and the cumulative volume frequency of the silica particles with a particle size of 15 nm is 20% or less.
Claim: 9. The method according to claim 7, wherein the silica particles are colloidal silica.
Claim: 10. The method according to claim 7, wherein the substrate to be polished is polished at a polishing pressure of 11.7 to 20 kPa in the polishing step.
Claim: 11. The method according to claim 7, further comprising a final polishing step of polishing the substrate to be polished at a polishing pressure of less than 11.7 kPa after polishing the substrate to be polished at a polishing pressure of 11.7 to 20 kPa in the polishing step.
Claim: 12. The method according to claim 7, wherein the silica particles have a value in the range of 100 to 130, and the value is obtained by dividing an area of a circle whose circumference is a perimeter of the silica particle by the projected area of the silica particle and multiplying the result by 100, when observed with a transmission electron microscope to measure the perimeter and the projected area of each particle.
Current U.S. Class: 451/60
Current International Class: 24; 24
Accession Number: edspap.20070254563
Database: USPTO Patent Applications
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Language:English