Gas-liquid chromatography-mass spectrometry of synthetic ceramides

Bibliographic Details
Title: Gas-liquid chromatography-mass spectrometry of synthetic ceramides
Authors: Bengt Samuelsson, Karin Samuelsson
Source: Journal of Lipid Research, Vol 10, Iss 1, Pp 41-46 (1969)
Publisher Information: Elsevier, 1969.
Publication Year: 1969
Collection: LCC:Biochemistry
Subject Terms: trimethylsilyl ethers, sphingosine, sphinganine, Biochemistry, QD415-436
More Details: Two series of ceramides with either sphingosine (sphing-4-enine) or sphinganine as base and with one of the saturated fatty acids C16, C18, C20, C22, C24, C26, or oleic acid were analyzed as the 1,3-di-O-trimethylsilyl ether derivatives by gas chromatography-mass spectrometry. The fragments formed on electron impact can be divided into three main groups, namely “molecular weight fragments,” “long-chain base fragments,” and “fatty acid fragments.” The m/e values of these fragments can be used to determine unequivocally the structures of the long-chain base and fatty acid of a ceramide derived from a sphingolipid.
Document Type: article
File Description: electronic resource
Language: English
ISSN: 0022-2275
Relation: http://www.sciencedirect.com/science/article/pii/S0022227520426471; https://doaj.org/toc/0022-2275
DOI: 10.1016/S0022-2275(20)42647-1
Access URL: https://doaj.org/article/b2a0abd745794135855a711c168049ad
Accession Number: edsdoj.b2a0abd745794135855a711c168049ad
Database: Directory of Open Access Journals
More Details
ISSN:00222275
DOI:10.1016/S0022-2275(20)42647-1
Published in:Journal of Lipid Research
Language:English