Bibliographic Details
| Title: |
N-Ethyl-2-[1-(2-hydroxy-4-methylphenyl)ethylidene]hydrazinecarbothioamide |
| Authors: |
Brian J. Anderson, Jeffrey R. Hall, Jerry P. Jasinski |
| Source: |
Acta Crystallographica Section E, Vol 70, Iss 6, Pp o735-o735 (2014) |
| Publisher Information: |
International Union of Crystallography, 2014. |
| Publication Year: |
2014 |
| Collection: |
LCC:Crystallography |
| Subject Terms: |
Crystallography, QD901-999 |
| More Details: |
The title compound, C12H17N3OS, crystallizes with two independent molecules (A and B) in the asymmetric unit. The dihedral angle between the mean planes of the benzene ring and the hydrazinecarbothioamide group are 6.9 (4) and 37.2 (5)° in molecules A and B, respectively. An intramolecular O—H...N hydrogen bond is observed in each molecule. This serves to maintain an approximately planar conformation for molecule A, but leaves a significant twist between these two groups in molecule B. In the crystal, a weak N—H...S interaction is observed, forming inversion dimers among the B molecules and resulting in an R22(8) motif. These dimers are further interconnected by weak N—H...O and C—H...O intermolecular interactions, forming chains along [011]. |
| Document Type: |
article |
| File Description: |
electronic resource |
| Language: |
English |
| ISSN: |
1600-5368
16005368 |
| Relation: |
http://scripts.iucr.org/cgi-bin/paper?S1600536814012203; https://doaj.org/toc/1600-5368 |
| DOI: |
10.1107/S1600536814012203 |
| Access URL: |
https://doaj.org/article/5269c6834daf46dabf94a0d5daf85a28 |
| Accession Number: |
edsdoj.5269c6834daf46dabf94a0d5daf85a28 |
| Database: |
Directory of Open Access Journals |
