Determination of chlorantraniliprole and penoxsulam residues in rice by QuEChERS-UPLC-MS/MS
| Title: | Determination of chlorantraniliprole and penoxsulam residues in rice by QuEChERS-UPLC-MS/MS |
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| Authors: | HUANG Zijie, HUANG Pengmian, LUO Kuanneng, XIANG Zhongping, ZHANG Honggang |
| Source: | Shipin yu jixie, Vol 40, Iss 1, Pp 63-67 (2024) |
| Publisher Information: | The Editorial Office of Food and Machinery, 2024. |
| Publication Year: | 2024 |
| Collection: | LCC:Food processing and manufacture |
| Subject Terms: | quechers, chlorantraniliprole, penoxsulam, rice, residue, Food processing and manufacture, TP368-456 |
| More Details: | Objective: To establish a new QuEChERS-ultra-performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS) method for the detection of chlorantraniliprole and penoxsulam residues in rice. Methods: After the sample was extracted with 0.2% formic acid-acetonitrile, purified with N-propylethylenediamine (PSA) and graphitized carbon black (GCB) packing, 0.2% formic acid water and acetonitrile were used as mobile phases for gradient elution, and then subjected to C18 chromatography. UPLC-MS/MS was used to column separation and determination. Results: The limits of quantification (LOQ) of chlorantraniliprole and penoxsulam were both 0.004 mg/kg, and the method detection limits (LOD) were both 0.001 mg/kg. Chlorantraniliprole and penoxsulam had a good linear relationship in the range of 0.002~0.5 mg/L, and their coefficient was greater than 0.993. At the addition levels of 0.05, 0.1, and 0.5 mg/kg, the average recovery rates of chlorantraniliprole and penoxsulam were 86% to 110% with the relative standard deviations (RSD) of 1.5% to 6.1%. Conclusion: This method is efficient and simple, has good stability and high sensitivity, and is suitable for the detection of chlorantraniliprole and penoxsulam in rice. |
| Document Type: | article |
| File Description: | electronic resource |
| Language: | English Chinese |
| ISSN: | 1003-5788 |
| Relation: | http://www.ifoodmm.com/spyjxen/article/abstract/20240110; https://doaj.org/toc/1003-5788 |
| DOI: | 10.13652/j.spjx.1003.5788.2023.80822 |
| Access URL: | https://doaj.org/article/43aa6e2e980b44b585cfa1b6abfad4d7 |
| Accession Number: | edsdoj.43aa6e2e980b44b585cfa1b6abfad4d7 |
| Database: | Directory of Open Access Journals |
| ISSN: | 10035788 |
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| DOI: | 10.13652/j.spjx.1003.5788.2023.80822 |
| Published in: | Shipin yu jixie |
| Language: | English Chinese |