Ultrafine-grained LaB6–ZrB2 composite ceramics with superior mechanical and thermionic emission properties prepared by high-pressure sintering

Bibliographic Details
Title: Ultrafine-grained LaB6–ZrB2 composite ceramics with superior mechanical and thermionic emission properties prepared by high-pressure sintering
Authors: Xiaogang Guo, An Liu, Lingjuan Hao, Hang Zhou, Shuai Chen, Pan Ying, Bing Liu, Baozhong Li, Yufei Gao, Zhisheng Zhao, Ling Kong, Mengdong Ma, Xinyu Yang, Dongli Yu
Source: Journal of Advanced Ceramics, Vol 13, Iss 12, Pp 2021-2029 (2024)
Publisher Information: Tsinghua University Press, 2024.
Publication Year: 2024
Collection: LCC:Clay industries. Ceramics. Glass
Subject Terms: lab6–zrb2, ultrafine-grained, high pressure, mechanical properties, thermal field emission, Clay industries. Ceramics. Glass, TP785-869
More Details: In this study, ultrafine-grained LaB6–ZrB2 composite ceramics were successfully synthesized by sintering a mixture of self-produced LaB6 nanopowder and commercial ZrB2 nanopowder under high pressure. Compared with their coarse-grained counterparts, ultrafine-grained ceramics exhibit improved mechanical properties. Notably, the ultrafine-grained LaB6–ZrB2 composite ceramic sintered at 4 GPa and 1673 K, with an average grain size of 286 nm, shows optimal mechanical performance characterized by a Vickers hardness of 25.6 GPa, a fracture toughness of 4.1 MPa·m1/2, and an elastic modulus of 338 GPa. Furthermore, the ultrafine-grained LaB6–ZrB2 composite ceramics displayed strong thermal emission, reaching a maximum current density of 27.5 A∙cm−2 at 1773 K. The structural and functional advantages of ultrafine-grained LaB6–ZrB2 composite ceramics render them suitable for potential use in thermionic emission cathodes.
Document Type: article
File Description: electronic resource
Language: English
ISSN: 2226-4108
2227-8508
Relation: https://www.sciopen.com/article/10.26599/JAC.2024.9220995; https://doaj.org/toc/2226-4108; https://doaj.org/toc/2227-8508
DOI: 10.26599/JAC.2024.9220995
Access URL: https://doaj.org/article/c32ab3ac64824d0fb6bf50f8f13ebff9
Accession Number: edsdoj.32ab3ac64824d0fb6bf50f8f13ebff9
Database: Directory of Open Access Journals
More Details
ISSN:22264108
22278508
DOI:10.26599/JAC.2024.9220995
Published in:Journal of Advanced Ceramics
Language:English