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Simultaneous evaluation and monitoring ochratoxin A, aflatoxins, and zearalenone contamination levels of cereals from Iranian retail market using HPLC-FLD: A 3-year survey

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Title: Simultaneous evaluation and monitoring ochratoxin A, aflatoxins, and zearalenone contamination levels of cereals from Iranian retail market using HPLC-FLD: A 3-year survey
Authors: Fatemeh Kardani, Aniseh Zarei Jelyani, Marzieh Rashedinia, Saeedeh Shariati, Mohammad Hashemi, Seyyed Mohammad Ali Noori, Masoud Mahdavinia
Source: Food Chemistry Advances, Vol 3, Iss , Pp 100490- (2023)
Publisher Information: Elsevier, 2023.
Publication Year: 2023
Collection: LCC:Food processing and manufacture
Subject Terms: HPLC, Aflatoxins, Ochratoxin A, Zearalenone, Cereals, Food processing and manufacture, TP368-456
More Details: Mycotoxins are important for farmers and public health. Due to the widespread use of cereals around the world, their monitoring is of great importance. In this study, the simultaneous determination and analysis of aflatoxins (AFs), ochratoxin A (OTA), and zearalenone (ZEN) in Iranian cereal samples, including 150 rice, 150 wheat, and 150 corn samples, were carried out using an immunoaffinity column and analyzed using HPLC-FLD. Under the optimal conditions, the linear range was 0.01–30, 0.03–40 and 0.2–350 ng g-1 for AFs, OTA, and ZEN, respectively. The detection of limit was between 0.0028–0.0035, 0.015 and 0.061 ng g−1, and the qualitative of limit was between 0.0093–0.015, 0.052 and 0.203 for AF, OTA, and ZEN, respectively. In conclusion from the 450 cereal samples, only 7 % contained mycotoxins, and the maximum residue limit (MRL) were less than 1 %. These results show that grain products in Iran are well controlled by the Health and Food and Drug Organization.
Document Type: article
File Description: electronic resource
Language: English
ISSN: 2772-753X
Relation: http://www.sciencedirect.com/science/article/pii/S2772753X23003118; https://doaj.org/toc/2772-753X
DOI: 10.1016/j.focha.2023.100490
Access URL: https://doaj.org/article/dcd716e997894a439962893a83055594
Accession Number: edsdoj.716e997894a439962893a83055594
Database: Directory of Open Access Journals
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  Data: Simultaneous evaluation and monitoring ochratoxin A, aflatoxins, and zearalenone contamination levels of cereals from Iranian retail market using HPLC-FLD: A 3-year survey
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  Data: <searchLink fieldCode="AR" term="%22Fatemeh+Kardani%22">Fatemeh Kardani</searchLink><br /><searchLink fieldCode="AR" term="%22Aniseh+Zarei+Jelyani%22">Aniseh Zarei Jelyani</searchLink><br /><searchLink fieldCode="AR" term="%22Marzieh+Rashedinia%22">Marzieh Rashedinia</searchLink><br /><searchLink fieldCode="AR" term="%22Saeedeh+Shariati%22">Saeedeh Shariati</searchLink><br /><searchLink fieldCode="AR" term="%22Mohammad+Hashemi%22">Mohammad Hashemi</searchLink><br /><searchLink fieldCode="AR" term="%22Seyyed+Mohammad+Ali+Noori%22">Seyyed Mohammad Ali Noori</searchLink><br /><searchLink fieldCode="AR" term="%22Masoud+Mahdavinia%22">Masoud Mahdavinia</searchLink>
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  Data: Food Chemistry Advances, Vol 3, Iss , Pp 100490- (2023)
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  Data: Mycotoxins are important for farmers and public health. Due to the widespread use of cereals around the world, their monitoring is of great importance. In this study, the simultaneous determination and analysis of aflatoxins (AFs), ochratoxin A (OTA), and zearalenone (ZEN) in Iranian cereal samples, including 150 rice, 150 wheat, and 150 corn samples, were carried out using an immunoaffinity column and analyzed using HPLC-FLD. Under the optimal conditions, the linear range was 0.01–30, 0.03–40 and 0.2–350 ng g-1 for AFs, OTA, and ZEN, respectively. The detection of limit was between 0.0028–0.0035, 0.015 and 0.061 ng g−1, and the qualitative of limit was between 0.0093–0.015, 0.052 and 0.203 for AF, OTA, and ZEN, respectively. In conclusion from the 450 cereal samples, only 7 % contained mycotoxins, and the maximum residue limit (MRL) were less than 1 %. These results show that grain products in Iran are well controlled by the Health and Food and Drug Organization.
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