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Investigation of Phase Formation in Ceramic Based on Zn, Sn, and Ti Oxides.

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Title: Investigation of Phase Formation in Ceramic Based on Zn, Sn, and Ti Oxides.
Authors: Zeer, G. M.1 (AUTHOR) gzeer@sfu-kras.ru, Zelenkova, E. G.1 (AUTHOR), Shubin, A. A.1 (AUTHOR), Abkaryan, A. K.1 (AUTHOR), Beletskii, V. V.1 (AUTHOR)
Source: Glass & Ceramics. Mar2023, Vol. 79 Issue 11/12, p507-511. 5p.
Subject Terms: *ZINC tin oxide, *CERAMICS, *TIN, *OXIDE ceramics, *ELECTRON microscopy, *OXIDES
Abstract: Solid-phase sintering was used to make ceramic from a mixture of ZnO, SnO2, and TiO2 nanopowders used as precipitation-strengthening and arc-quenching components in silver-based electrocontact materials. The phase formation and microstructure of the resulting material were studied by electron microscopy, energy-dispersive microanalysis, and x-ray phase analysis. It was found that a dispersed structure of size 0.5 – 1.0 μm forms from the Zn2TiO4 and ZnO phases at sintering temperature 1123 K, and the samples have quite high porosity. Solid-phase reactions in the ZnO/TiO2 system at Tsint = 1123 K effect the formation of two-phase ZnO/Zn2TiO4 ceramic with zinc and tin oxide phases in residual amounts. At sintering temperature 1443 K grain growth occurs, Zn2SnO4 becomes the predominant phase, and a certain amount of zinc and tin oxide phases remains. There is no manifestations of titanium-containing phases (presumably TiO2 and Zn2TiO4), probably because of their low content. [ABSTRACT FROM AUTHOR]
Copyright of Glass & Ceramics is the property of Springer Nature and its content may not be copied or emailed to multiple sites or posted to a listserv without the copyright holder's express written permission. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)
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  Group: Ti
  Data: Investigation of Phase Formation in Ceramic Based on Zn, Sn, and Ti Oxides.
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  Data: <searchLink fieldCode="JN" term="%22Glass+%26+Ceramics%22">Glass & Ceramics</searchLink>. Mar2023, Vol. 79 Issue 11/12, p507-511. 5p.
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  Data: *<searchLink fieldCode="DE" term="%22ZINC+tin+oxide%22">ZINC tin oxide</searchLink><br />*<searchLink fieldCode="DE" term="%22CERAMICS%22">CERAMICS</searchLink><br />*<searchLink fieldCode="DE" term="%22TIN%22">TIN</searchLink><br />*<searchLink fieldCode="DE" term="%22OXIDE+ceramics%22">OXIDE ceramics</searchLink><br />*<searchLink fieldCode="DE" term="%22ELECTRON+microscopy%22">ELECTRON microscopy</searchLink><br />*<searchLink fieldCode="DE" term="%22OXIDES%22">OXIDES</searchLink>
– Name: Abstract
  Label: Abstract
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  Data: Solid-phase sintering was used to make ceramic from a mixture of ZnO, SnO2, and TiO2 nanopowders used as precipitation-strengthening and arc-quenching components in silver-based electrocontact materials. The phase formation and microstructure of the resulting material were studied by electron microscopy, energy-dispersive microanalysis, and x-ray phase analysis. It was found that a dispersed structure of size 0.5 – 1.0 μm forms from the Zn2TiO4 and ZnO phases at sintering temperature 1123 K, and the samples have quite high porosity. Solid-phase reactions in the ZnO/TiO2 system at Tsint = 1123 K effect the formation of two-phase ZnO/Zn2TiO4 ceramic with zinc and tin oxide phases in residual amounts. At sintering temperature 1443 K grain growth occurs, Zn2SnO4 becomes the predominant phase, and a certain amount of zinc and tin oxide phases remains. There is no manifestations of titanium-containing phases (presumably TiO2 and Zn2TiO4), probably because of their low content. [ABSTRACT FROM AUTHOR]
– Name: AbstractSuppliedCopyright
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  Data: <i>Copyright of Glass & Ceramics is the property of Springer Nature and its content may not be copied or emailed to multiple sites or posted to a listserv without the copyright holder's express written permission. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.</i> (Copyright applies to all Abstracts.)
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        Text: English
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              Text: Mar2023
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