Control of Hydrogen Fluoride Formation and Release during a Large-Scale Nitroarene Reduction in the Manufacture of AZD9977

Authors: Mallia, Carl J., Le Bars, Joël, Hardy, Simon, Lamacraft, Alex, Harding, Simon, Hose, David, Snow, Lindsay, Poulten, Rebecca C., Dobson, Benjamin C., Churchill, Trevor

Source: Organic process research & development. 27(1):167-178

Availability: http://explore.bl.uk/primo_library/libweb/action/display.do?tabs=detailsTab&gathStatTab=true&ct=display&fn=search&doc=ETOCRN631627983&indx=1&recIds=ETOCRN631627983

Towards improved characterisation of complex polyethylene glycol excipients using supercritical fluid chromatography-evaporative light scattering detection-mass spectrometry and comparison with size exclusion chromatography-triple detection array

Authors: Poulton, Andrew M, Poulten, Rebecca C, Baldaccini, Alice, Gabet, Anaëlle, Mott, Rebecca, Treacher, Kevin E, Roddy, Emily, Ferguson, Paul

Source: In Journal of Chromatography A 8 February 2021 1638

This result is not displayed to guests.
Login for full access.

This result is not displayed to guests.
Login for full access.

Mono- and dinuclear Ni(i) products formed upon bromide abstraction from the Ni(i) ring-expanded NHC complex [Ni(6-Mes)(PPh3)Br].

Authors: Blackaby, William J. M., Sabater, Sara, Poulten, Rebecca C., Page, Michael J., Folli, Andrea, Krewald, Vera, Mahon, Mary F., Murphy, Damien M., Richards, Emma, Whittlesey, Michael K.

Source: Dalton Transactions: An International Journal of Inorganic Chemistry; 1/22/2018, Vol. 47 Issue 3, p769-782, 14p

Subject Terms: METAL complexes, BROMIDES, PHOSPHINE, ABSTRACTION reactions, CHEMICAL yield, SODIUM salts

This result is not displayed to guests.
Login for full access.

This result is not displayed to guests.
Login for full access.

This result is not displayed to guests.
Login for full access.

This result is not displayed to guests.
Login for full access.

This result is not displayed to guests.
Login for full access.

This result is not displayed to guests.
Login for full access.

This result is not displayed to guests.
Login for full access.

This result is not displayed to guests.
Login for full access.

Mechanistic Studies of the Rhodium NHC Catalyzed Hydrodefluorinationof Polyfluorotoluenes.

Authors: Schwartsburd, Leonid, Mahon, Mary F., Poulten, Rebecca C., Warren, Mark R., Whittlesey, Michael K.

Source: Organometallics; Nov2014, Vol. 33 Issue 21, p6165-6170, 6p

Rh–FHF and Rh–F Complexes ContainingSmall N-Alkyl Substituted Six-Membered RingN-Heterocyclic Carbenes.

Authors: Bramananthan, Nicola, Carmona, María, Lowe, John P., Mahon, Mary F., Poulten, Rebecca C., Whittlesey, Michael K.

Source: Organometallics; Apr2014, Vol. 33 Issue 8, p1986-1995, 10p

Synthesis, Electronic Structure, and Magnetism of [Ni(6-Mes)2]⁺: A Two-Coordinate Nickel(I) Complex Stabilized by Bulky N-Heterocyclic Carbenes.

Authors: Poulten, Rebecca C.¹, Page, Michael J.¹, Algarra, Andrés G.², Le Roy, Jennifer J.³, López, Isidoro⁴, Carter, Emma⁵, Llobet, Antoni⁵, Macgregor, Stuart A.¹, Mahon, Mary F.¹, Murphy, Damien M.⁵, Murugesu, Muralee², Whittlesey, Michael K.¹, m.k.whittlesey@bath.ac.uk

Source: Journal of the American Chemical Society; 9/18/2013, Vol. 135 Issue 37, p13640-13643, 4p

Synthesis and Small Molecule Reactivity of trans-Dihydride Isomers of Ru(NHC)2(PPh3)2H2(NHC = N-Heterocyclic Carbene).

Authors: Davies, Caroline J. E., Lowe, John P., Mahon, Mary F., Poulten, Rebecca C., Whittlesey, Michael K.

Source: Organometallics; Vol. 32 Issue 17, p4927-4937, 11p

Ring-Expanded N-HeterocyclicCarbene Complexes of Rhodium with Bifluoride, Fluoride, and FluoroarylLigands.

Authors: Segarra, Candela, Mas-Marzá, Elena, Lowe, John P., Mahon, Mary F., Poulten, Rebecca C., Whittlesey, Michael K.

Source: Organometallics; Vol. 31 Issue 24, p8584-8590, 7p

This result is not displayed to guests.
Login for full access.