Comparison of Different Approaches for Calculating LOD and LOQ in an HPLC-Based Analysis Method

Authors: Raha Kaviani

Source: Pharmaceutical Sciences, Vol 31, Iss 1, Pp 106-109 (2025)

Subject Terms: analytical method validation, lod, loq, pharmaceutical analysis, sensitivity, Pharmacy and materia medica, RS1-441

File Description: electronic resource

Relation: https://ps.tbzmed.ac.ir/PDF/ps-31-106.pdf; https://doaj.org/toc/2383-2886

Access URL: https://doaj.org/article/3589667f32894239ac68a8061b00829e

A high-performance thin-layer chromatography densitometric method for the separation of isomeric ceftriaxone in powder for injection formulation

Authors: Kissa W. Mwamwitwa, Bugusu Nyamweru, Mohamed A. Iwodyah, Gerald Sambu, Goodluck G. Nyondo, Emili Yondu, Adam M. Fimbo, Vicky Manyanga, Wilber Sabiiti, Danstan H. Shewiyo, Morven C. Shearer, Andrew D. Smith, Eliangiringa A. Kaale

Source: Scientific Reports, Vol 14, Iss 1, Pp 1-9 (2024)

Subject Terms: Ceftriaxone Sodium, Isomers, High performance thin layer chromatography, Analytical method validation, Medicine, Science

File Description: electronic resource

Relation: https://doaj.org/toc/2045-2322

Access URL: https://doaj.org/article/b3b890b36f6a4b52b75890d6d52ca79a

Evaluation of acrolein content in food products from South Korea using LC-MS/MS

Authors: Kyung-Jik Lim, Han-Seung Shin

Source: Journal of Agriculture and Food Research, Vol 19, Iss , Pp 101550- (2025)

Subject Terms: Acrolein, LC-MS/MS, Agricultural foods, Non-thermal contaminants, Analytical method validation, Hazardous, Agriculture (General), S1-972, Nutrition. Foods and food supply, TX341-641

File Description: electronic resource

Relation: http://www.sciencedirect.com/science/article/pii/S2666154324005878; https://doaj.org/toc/2666-1543

Access URL: https://doaj.org/article/d3c4ea027bab4587bb7e14b1269b0317

Determination of carbon dioxide by gas chromatography using an electron capture detector for the analysis of greenhouse gases: A comparison and validation with the standard method

Authors: Arias, Joan Noguerol ^⁎, Bonmatí, August, Prenafeta-Boldú, Francesc X., Cerrillo, Míriam

Source: In Journal of Chromatography A 29 March 2025 1745

Overcoming challenges in the analysis of the ubiquitous emerging contaminant trifluoroacetic acid employing trap column liquid chromatography tandem mass spectrometry

Authors: Sayed, Ramadan ^{a, b, ⁎, 1}, Omran, Ahmed A. ^a, Farag, Rabie S. ^a, Mahmoud, Hend A. ^b, Soliman, Mostafa ^{b, ⁎⁎, 2}

Source: In Journal of Hazardous Materials 5 July 2025 491

QbD and green metric based HPLC method development and validation of bromocriptine mesylate in bulk product and biological samples

Authors: Saini, Sumant ^{a, b}, Kaur, Ripandeep ^{b, c}, Kaur, Ranjot ^b, Gulati, Monica ^a, Singh, Bhupinder ^{b, c, d, ⁎⁎}, Hussain, Afzal ^e, Ahad, Abdul ^e, Ramzan, Mohhammad ^{a, ⁎}, Shahid, Mudassar ^e, Ayub, Arusha ^f

Source: In Journal of Chromatography B 15 May 2025 1258

A novel HPLC method for simultaneous estimation of natamycin and voriconazole for ocular drug delivery applications

Authors: Kailasam, Velmurugan, Dasgupta, Oindrilla, Mannangatty, Tamizhmathy, Nirmal, Jayabalan ^⁎

Source: In Journal of Pharmaceutical and Biomedical Analysis 15 May 2025 257

Projection Profiling: A Data Compressing Strategy in Three-Dimensional Liquid Chromatography for Quality Control of Traditional Herbal Medicine

Authors: Jing Zhang

Source: Sensors, Vol 25, Iss 7, p 2015 (2025)

Subject Terms: projection profiling, baseline correction, analytical method validation, traditional herbal medicine, quality control, Chemical technology, TP1-1185

File Description: electronic resource

Relation: https://www.mdpi.com/1424-8220/25/7/2015; https://doaj.org/toc/1424-8220

Access URL: https://doaj.org/article/7a4862dc32fa4af08a3fb14feed81f57

A Quantitative Approach to Potency Testing for Chimeric Antigen Receptor-Encoding Lentiviral Vectors and Autologous CAR-T Cell Products, Using Flow Cytometry

Authors: Juan José Mata-Molanes, Leticia Alserawan, Carolina España, Carla Guijarro, Ana López-Pecino, Hugo Calderón, Ane Altuna, Lorena Pérez-Amill, Nela Klein-González, Carlos Fernández de Larrea, Europa Azucena González-Navarro, Julio Delgado, Manel Juan, Maria Castella

Source: Pharmaceutics, Vol 17, Iss 3, p 303 (2025)

Subject Terms: chimeric antigen receptor, potency testing, T-cell activation, analytical method validation, ATMP development, Pharmacy and materia medica, RS1-441

File Description: electronic resource

Relation: https://www.mdpi.com/1999-4923/17/3/303; https://doaj.org/toc/1999-4923

Access URL: https://doaj.org/article/d3480d402c6d424bacbefa8e9b330a8b

Determination of zinc content in insulin products by inductively coupled plasma mass spectrometry

Authors: Yu. N. Shvetsova, A. A. Erina, E. A. Khorolskaya, E. S. Zhigilei, N. E. Kuz’mina

Source: Регуляторные исследования и экспертиза лекарственных средств, Vol 13, Iss 3, Pp 394-402 (2023)

Subject Terms: zinc, insulin, analytical method validation, inductively coupled plasma mass spectrometry, icp-ms, flame atomic absorption spectrometry, faas, Medicine (General), R5-920

File Description: electronic resource

Relation: https://www.vedomostincesmp.ru/jour/article/view/558; https://doaj.org/toc/3034-3062; https://doaj.org/toc/3034-3453

Access URL: https://doaj.org/article/66dbf859792942679a148519eeb451f9

Chromatographic Analysis of Pesticide in Environmental and Food

Contributors: González-Curbelo, Miguel Ángel

Subject Terms: green extraction techniques, sample preparation, clean-up, multiresidue analysis, environmentally friendly methods, flupyradifurone, ginseng, analytical method, mass spectrometry, pesticide residue analysis, in situ coacervative extraction, double-solvent supramolecular system, triazole fungicides, extraction, HPLC, cyclaniliprole, diamide insecticide, residue analysis, DPX, UHPLC-MS/MS, pesticide residues, vegetables, fruits, dietary risk exposure, compound-specific isotope analysis, pollutant, agricultural application, soil, SPE extraction, analytical method validation, chromatography, food safety, polar pesticides, risk assessment, quality control procedures, sources of errors of residue analyses, reproducibility of results, antifouling biocides, high-performance liquid chromatography–mass spectrometry (LC-MS), ionic liquid-dispersive liquid–liquid micro-extraction (IL-DLLME), QuEChERS, EDIs, ADI, HRI, GC–MS/MS, LC-MSMS, pesticides, toxins, cereals, LC-MS/MS, screening, validation, herbal decoction, traditional Korean medicine, QuPPe, proso millet, determination, LC–MS/MS, phase-transfer purification, carrageenan, carbamate pesticides, isoxaflutole, atrazine, terminal residues, dietary risk assessment, Research and information: general, Chemistry, Analytical chemistry

File Description: application/octet-stream

Access URL: https://directory.doabooks.org/handle/20.500.12854/128758
https://mdpi.com/books/pdfview/book/8223

Extraction method for the multiresidue analysis of legacy and emerging pollutants in marine mussels from the Adriatic Sea

Authors: Interino, Nicolò ^{a, 1}, Comito, Rossana ^{a, 1}, Simoni, Patrizia ^b, Franzellitti, Silvia ^c, Palladino, Giorgia ^d, Rampelli, Simone ^d, Mosendz, Anastasiia ^e, Gotti, Roberto ^d, Roda, Aldo ^{a, f}, Candela, Marco ^d, Porru, Emanuele ^{b, ⁎}, Fiori, Jessica ^{a, ⁎}

Source: In Food Chemistry 1 November 2023 425

Development and validation of a versatile analytical method for absolute quantification of seven oligosaccharides in human, bovine, and goat milk

Authors: Urrutia-Baca, Víctor H. ^a, Chuck-Hernández, Cristina ^a, Gutiérrez-Uribe, Janet ^a, Ramos-Parra, Perla A. ^{b, ∗}, Licona-Cassani, Cuauhtemoc ^{a, b}

Source: In Heliyon November 2023 9(11)

Development and validation of a peptide-mapping procedure for a novel C1 esterase inhibitor

Authors: E. V. Zubareva, M. D. Degterev, M. Yu. Neronova, M. A. Smolov, R. R. Shukurov

Source: Биопрепараты: Профилактика, диагностика, лечение, Vol 23, Iss 2, Pp 203-218 (2023)

Subject Terms: c1 esterase inhibitor, recombinant protein, analytical method validation, peptide mapping, rp-hplc, Biotechnology, TP248.13-248.65, Medicine

File Description: electronic resource

Relation: https://www.biopreparations.ru/jour/article/view/461; https://doaj.org/toc/2221-996X; https://doaj.org/toc/2619-1156

Access URL: https://doaj.org/article/4af3fc9c5432473baaf7e09c1477bfdb

Development and validation of an LC-MS/MS method to quantify ceftaroline in microdialysate samples from plasma and brain: Application to a preclinical pharmacokinetic investigation

Authors: Helfer, Victória Etges ^a, Dias, Bruna Bernar ^a, Lock, Graziela de Araújo ^a, Tomaszewski, Caroline Andrade ^b, Barnet, Lucas Suchecki ^b, Barreto, Fabiano ^b, Zavascki, Alexandre Prehn ^{c, d}, Araújo, Bibiana Verlindo de ^a, Dalla Costa, Teresa ^{a, ∗}

Source: In Heliyon June 2023 9(6)

Accurate low-dose exposure assessment of benzene and monoaromatic compounds by diffusive sampling: sampling and analytical method validation according to ISO 23320 for radiello® samplers packed with activated charcoal

Authors: Laura Zaratin, Caterina Boaretto, Riccardo Carnevale Schianca, George Hinkal, Elena Grignani, Danilo Cottica

Source: Frontiers in Public Health, Vol 11 (2023)

Subject Terms: benzene, inhalation exposure assessment, sampling and analytical method validation, gasoline vapors, hexane, isopropyl benzene, Public aspects of medicine, RA1-1270

File Description: electronic resource

Relation: https://www.frontiersin.org/articles/10.3389/fpubh.2023.1271550/full; https://doaj.org/toc/2296-2565

Access URL: https://doaj.org/article/bef5d5972fa346039bfbdabcb63f78c3

Development and validation of chemometric-assisted spectrophotometric method for the simultaneous estimation of aceclofenac, paracetamol, and chlorzoxazone with impurities

Authors: Rajshree Gunjal, Arti Gajbhar, Vijaya Vichare, Abhijeet Sutar, Minal Deshmukh, Vishnu Choudhari

Source: Biomedical and Biotechnology Research Journal, Vol 6, Iss 3, Pp 458-465 (2022)

Subject Terms: aceclofenac, analytical method validation, chemometric, chlorzoxazone, impurities, paracetamol, partial least square, principal component regression, spectrophotometric, Biotechnology, TP248.13-248.65

File Description: electronic resource

Relation: http://www.bmbtrj.org/article.asp?issn=2588-9834;year=2022;volume=6;issue=3;spage=458;epage=465;aulast=Gunjal; https://doaj.org/toc/2588-9834; https://doaj.org/toc/2588-9842

Access URL: https://doaj.org/article/2f9504fea3244e98ad5e7627eabd5bf7

Spectrophotometric simultaneous analytical method validation to determine isoniazid and pyridoxine in pure and 3D printed tablet forms

Authors: Nur Suhaila Sudarman, Muhammad Salahuddin Haris

Source: Journal of Pharmacy, Vol 3, Iss 1 (2023)

Subject Terms: Isoniazid, pyridoxine, UV-Vis spectrophotometer, simultaneous equation method, analytical method validation, Pharmacy and materia medica, RS1-441

File Description: electronic resource

Relation: https://journals.iium.edu.my/ktn/index.php/jp/article/view/176; https://doaj.org/toc/2773-5664

Access URL: https://doaj.org/article/d0aede7dc7e24383850186f0cf258443

A Validated HPLC-UV-ESI-IT-MS Method for the Quantification of Carnosol in Lepechinia mutica, a Medicinal Plant Endemic to Ecuador

Authors: Natalí Solano-Cueva, Jorge G. Figueroa, Corina Loja, Chabaco Armijos, Giovanni Vidari, Jorge Ramírez

Source: Molecules, Vol 28, Iss 18, p 6701 (2023)

Subject Terms: carnosol, Lepechinia mutica, HPLC-UV-ESI-IT-MS analysis, analytical method validation, Organic chemistry, QD241-441

File Description: electronic resource

Relation: https://www.mdpi.com/1420-3049/28/18/6701; https://doaj.org/toc/1420-3049

Access URL: https://doaj.org/article/995512b297c1467393269a03343dff4c

Selenium Isotope Studies in Plants - Development and Validation of a Novel Geochemical Tool and its Application to Organic Samples

Authors: Banning, Helena

Subject Terms: GN301-674, analytical method validation, Selen in Pflanzen, HG-MC-ICP-MS-Analytik, HG-MC-ICP-MS analytics, Präparation organischer Umweltproben, selenium in plants, organic sample preparation, Stabile Isotope, Validierung analytischer Methodenselenium stable isotopes, Social & cultural anthropology, ethnography, Social and cultural anthropology

File Description: image/jpeg

Relation: Karlsruher mineralogische und geochemische Hefte : Schriftenreihe des Instituts für Angewandte Geowissenschaften

Access URL: https://directory.doabooks.org/handle/20.500.12854/59176
https://www.ksp.kit.edu/9783731505945